NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2 701\30352.D Vial: 19
Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Dec 31 12:15 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title ': 209 625/TCLP calibration table
Last Update : Fri Dec 14 12:19:30 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 986207 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 3787361 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 1933984 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 2867164m 20.00 ug/1 -0.01
38) Chrysene-dl2 33.02 240 1852221 20.00 ug/1 -0.01
44) Perylene-dl2 37.12 264 1120907 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 194805 4.69 ug/mL -0.01
Spiked Amount 5.000 Recovery = 93.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.56 74 230 N.D.
3) bis(2-Chloroethyl)ether 11.16 93 1438 N.D.
4) 1,3-Dichlorobenzene 11.61 146 1244 N.D. '
5) 1,4-Dichlorobenzene . 11.72 146 1427 N.D.
6) 1,2-Dichlorobenzene 12.26 146 1250 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 373 N.D.
11) Nitrobenzene 13.52 77 459 N.D.
12) 1sophorone 14.07 82 1064 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 15.19 180 488 N.D.
15) Naphthalene 15.34 128 5573 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.93 162 933 N.D.
20) Dimethylphthalate 20.02 163 3450 N.D.
21) 2,6-Dinitrotoluene 20.27 165 327 N.D.
22) Acenaphthylene 20.12 152 1818 N.D.
2 3) Acenaphthene 20.65 153 1839 N.D.
24) 2,4-Dinitrotoluene 21.33 165 298 N.D.
25) Diethylphthalate 22.11 149 5984 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
2 7) Fluorene 22.23 166 1300 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30352.D GCMS1126.M Mon Dec 31 12:17:57 2001 Page 1
NYC-WTC_000017810
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