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GCMS analysis report for sample AD30902, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.

NYC-WTC_000017615–000017629

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document , LSC Area Percent Report ‘Data File : M:\INSTRU~1\209\DATA\JAN0802\30902.D Vial: 20 Acq On : 9 Jan 2002) 7:51 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator, Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.470 260 264 277 rBV 305131 851095 12.78% 2.309% 2 7.608 277 279 297 rVB2 32303 140208 2.10% 0.380% 3 11.528 701 706 727 rBV 1993048 5135220 77.09% 13.930% 4 14.172 985 994 1000 rBV 252249 500320 7.51% 1.357% 5 15.117 1092 1097 1116 rBV 2934977 6395738 96.01% 17.350% 6 17.311 1328 1336 1344 rBV 427901 866912 13.01% 2.352% 7 18.000 1407 1411 1416 rBV 44478 85553 1.28% 0.232% 8 20.130 1637 1643 1650 rvB 294600 591089 8.87% 1.603% 9 20.387 1665 1671 1683 rBV 3080761 6661235 100.00% 18.070% 10 20.855 1717 1722 1734 rVB 236423 486572 7.30% 1.320% 11 22.636 1910 1916 1923 rBV 186552 359623 5.40% 0.976% 12 24.802 2146 2152 2165 rBV2 2996277 6590503 98.94% 17.878% 13 26.740 2357 2363 2368 rBV 64811 131452 1.97% 0.357% 14 28.502 2550 2555 2564 rvB 46086 95412 1.43% 0.259% 15 29.888 2700 2706 2712 rBV 349578 718179 10.78% 1.948% 16 30.090 2721 2728 2737 rBV 32028 70429 «1.06% 0.191% 17 32.835 3020 3027 3035 rBV2 1908380 4289104 64.39% 11.635% 18 36.902 3463 3470 3488 rBV2 1058513 2895288 43.46% 7.854% Sum of corrected areas: 36863932 30902.D GCMS0103.M Thu Jan 10 15:54:52 2002 . NYC-WTC_000017620

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NYC-WTC_000017620Source: NYC Law Department, mirrored locally

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