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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017600
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NYC 9/11 Public Portal Document . LSC Area Percent Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 * Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator! Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area max. total 1 7.465 260 264 277 rBvV 290500 807252 12.15% 2.109% 2 11.523 701 706 724 rBV 1865043 5024449 75.59% 13.128% 3 14.167 989 994 1000 rvB 316460 610882 9.19% 1.596% 4 15.121 1093 1098 1116 rBV 3004075 6195614 93.21% 16.187% 5 17.306 1328 1336 1344 rBV 666976 1287826 19.38% 3.365% 6 18.004 1407 1412 1417 rBV 75952 142460 2.14% 0.372% i 7 20.125 1638 1643 1649 rvB 497560 957402 14.40% 2.501% 8 20.391 1666 1672 1688 rBV 3178282 6539116 98.38% 17.085% 9 20.850 1717 1722 1738 rvB 352488 704184 10.59% 1.840% 10 22.640 1910 1917 1927 rBV 326225 631020 9.49% 1.649% 11 24.806 2147 2153 2166 rBV2 3131019 6646651 100.00% 17.366% 12 26.734 2357 2363 2369 rBV 140619 269920 4.06% 0.705% 13 28.497 2549 2555 2563 rVB -91744 191379 2.88% 0.500% 14 29.883 2701 2706 2714 rBV 337049 652428 99.82% 1.705% 15 30.094 2721 2729 2736 rBV 75554 161455 2.43% 0.422% 16 31.563 2883 2889 2899 rvB 51801 122259 1.84% 0.319% 17 32.839 3021 3028 3035 rBV2 1817993 4236979 63.75% 11.070% 18 32,931 3035 3038 3052 rvVB2 54669 162715 2.45% 0.425% 19 34.225 3172 3179 3188 rBV2 27197 76019 1.14% 0.199% 20 36.906 3464 3471 3489 rBV 1031764 2854102 42.94% 7.457% Sum of corrected areas: 38274112 . 31022.D GCMSO103.M Thu Jan 10 16:06:36 2002 NYC-WTC_000017600

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NYC-WTC_000017600Source: NYC Law Department, mirrored locally

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