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GCMS analysis results for sample AD29668, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29668 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036888–000036901

Folder label: “GCMS X 12/7/01 A 1/2/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘Data File : M:\INSTRU~l\209\DATA\DEC1301\29668.D Vial: 22 Acq On : 14 Dec 2001 5:24 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.595 274 278 290 rBV 410207 1041113 11.04% 2.126% 2 7.742 290 294 310 rVB 63080 235556 2.50% 0.481% 3 11.350 683 687 693 rBV 39046 101000 1.07% 0.206% 4 11.432 693 696 715 rVB 40253 138410 1.47% 0.283% 5 11.671 717 722 740 rBV 2659893 6766735 71.76% 13.819%

6 15.270 1109 1114 1133 rBV 3889209 8834584 93.69% 18.041% 7 20.549 1683 1689 1713 rBV 4194017 9429451 100.00% 19.256% 8 24.973 2164 2171 2183 rBV2 4040623 8862914 93.99% 18.099% 9 25.120 2183 2187 2200 rVB2 37944 134168 1.42% 0.274% 10 26.984 2386 2390 2396 rBV 48916 97188 1.03% 0.198%

11 30.050 2718 2724 2730 rBV 444213 906293 9.61% 1.851% 12 33.006 3037 3046 3064 rBV2 2853145 6843910 72.58% 13.976% 13 37.101 3484 3492 3514 rBV 1973415 5577155 59.15% 11.389%

Sum of corrected areas: 48968477

29668.D GCMS1126.M Tue Jan 08 10:58:32 2002

NYC-WTC_000036896

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NYC-WTC_000036896Source: NYC Law Department, mirrored locally

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