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GCMS analysis results for sample AD29734, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29734 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036874–000036887

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036882
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File M:\INSTRU~1\2O9\DATA\DEC13O1\29734.D Vial: 20 Acq On 14 Dec 2001 3:26 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 294 rBV 362354 935307 9.81% 1.949% 2 11.349 683 687 692 rBV 67280 164982 1.73% 0.344% 3 11.422 692 695 703 rVB 66216 173486 1.82% 0.361% 4 11.670 716 722 740 rBV 2947521 7084411 74.32% 14.760% 5 15.278 1109 1115 1133 rBV 4091182 8975278 94.15% 18.699%

6 20.557 1683 1690 1712 rBV 4282365 9532537 100.00% 19.860% 7 24.972 2165 2171 2184 rBV2 3930901 8862721 92.97% 18.464% 8 25.119 2184 2187 2200 rVB 36475 113862 1.19% 0.237% 9 30.049 2719 2724 2732 rBV 336261 684409 7.18% 1.426% 10 33.005 3036 3046 3072 rBV2 2621614 6527700 68.48% 13.600%

11 37.100 3484 3492 3513 rBV2 1705641 4944252 51.87% 10.301%

Sum of corrected areas: 47998945

29734.D GCMS1126.M Tue Jan 08 11:04:02 2002

NYC-WTC_000036882

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NYC-WTC_000036882Source: NYC Law Department, mirrored locally

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