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GCMS blank analysis results for sample AD30605, Jan 2002

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Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.

NYC-WTC_000017542–000017555

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File M: \INSTRU-1 \2 09\DATA\ JAN0 802 \LBB. D Vial: 18 Acq Oh 9 Jan 2002 5:55 am Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.466 260 264 279 rBV 342858 919900 14.74% 2.792% 2 11.000 644 649 658 rVB 105202 247291 3.96% 0.751% 3 11.523 701 706 729 rBV 1895827 4788810 76.72% 14.535% 4 14.167 989 994 1001 rVB 204728 383249 6.14% 1.163% 5 15.122 1093 1098 1117 rBV 2898877 5983764 95.87% 18.162%

6 17.307 1327 1336 1344 rVB 239752 462499 7.41% 1.404% 7 20.125 1635 1643 1648 rBV 146838 274856 4.40% 0.834% 8 20.392 1665 1672 1689 rBV 3029580 6241652 100.00% 18.945% 9 20.860 1718 1723 1734 rBV 64089 137296 2.20% 0.417%' 10 22.641 1911 1917 1923 rBV 74928 148629 2.38% 0.451% 11 24.807 2147 2153 2165 rBV2 2830180 5992006 96.00% 18.187% 12 29.884 2701 2706 2718 rVB 359326 700798 11.23% 2.127% 13 32.831 3021 3027 3049 rBV2 1656607 3932423 63.00% 11.936% 14 33.134 3055 3060 3068 rBV 52589 115663 1.85% 0.351% 15 36.907 3463 3471 3496 rBV 945763 2617343 41.93% 7.944%

Sum of corrected areas: 32946179

LBB.D GCMS0103.M Thu Jan 10 16:14:49 2002

NYC-WTC_000017546

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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