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GCMS analysis report for sample AD31021, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31021 conducted on January 18, 2002.

NYC-WTC_000017585–000017594

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017593
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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31021.D Vial: 22 Acq On : 9 dan 2002 10:47 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc 7 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L TEES ISIE EES EIIE IOI IE IOI IGG IS IST IEIO SS TOTOIE ISO IIIA TI IIIS Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. _EstConc Area Relative to ISTD R.T. 7.60 0.69 ug/l 180345 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 2-Propanong, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 45 2 N-Acetylpyrrolidone 127 C6HONO2 000932-17-2 5 3 2-AcetyYthiazole 127 C5H5NOS 024295-03-2 4 4 2-Acet#f1-1,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 Abundance ‘Scan 276 (7.600 ming: 31021.) m/z 43.05 100.00 | | |e | 35 | 49 55 61 82 99 sy7 125 7.20 740 7.60 7.80 8.00 | £8 Ce belt ripe | m/z 124.9 9.73 inz> 10.20 30. 40 50 60 70 80 @ 100 110 120 130 ‘Abundance #12247: 2-Propanone, 1,1.1-tichloro- | 5000: | 7.20 7.40 7.60 __7.80 _8.00 45 j m/z 46.9) 8.21 : 35 Ao 85. or 417 128 brvz> 40. 20.30 40. 50 60 70 80 0 100 110 120 130 Abundance fg Bae WAootreyratione | ae | 7.20 740 7.60 _7.80_8.00_| | 5000: m/z 81.9 7.42% 99 137 | 30 es oo 2d bia Oe bw ww OO 120 180 yurkdance ‘#4717: 2-Acetylthiazole | 7.20 7.40 7.80 7.80 _ 8.00. m/z 82.8, 6.99% a ea 99 427 ° i es | 112 | 33 I n> 10.20. 30. 40 50 60 70 80 0 100 110 120 130 | 7.20 740 7.60 7.80 800 31021.D GCMS0103.M Thu Jan 10 16:03:19 2002 Page 2 NYC-WTC_000017593

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NYC-WTC_000017593Source: NYC Law Department, mirrored locally

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