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GCMS unknowns analysis report for sample AD31340, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31340 using GCMS on February 11, 2002.

NYC-WTC_000017026–000017039

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017034
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0902\31340.D Vial: 7 Acq On : 10 Jan 2002 9:24 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eereeerrrrrrrrersr fst rere: rrrrrerrrrrrrrrrrrrtrrt ict iret iret torr irs Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.60 0.77 ug/l 127818 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 Tentative ID MW MolForm caASs# Qual 1 2-Propanone,, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 28 2 4-Penten-2-0one 84 C5H80 013891-87-7 9 3 N-Acetylpyrrolidone 127 CéH9No2 000932-17-2 5 4 2-acetyyehiazole 127_C5HS5NOS _ 024295-03-2 4 ‘Abundance ~ _. Sean 279 (7.603 min): 31340.0 ¢) m/z 42.95 100.004 | | | 5000- ] | | 125 7.20. 7.40 7.60 7.80 300 Be 9 |_7.20__7.40_7.60 7.80 _ 8.00 BB thus : m/z 124.9) 10.52% mizn-> __10 20 30 40 50 _60_70 _80 90 100 110 120 130 _ ‘Abundance #12247; 2-Propanone, 1.1,1-irichioro- | . | ] | seed | 7.20740 7.80 7.80. '8.00' | a m/z 96.95 7.04 85 128 35 Ao oe 7, 117 | mz 10_20 30 40 50 6 70 80 90 100 110 120 130 | Abundance BEE Fron oe | 43 | 7.20 __740__7.60__7.80__8.00 5000 m/z 127.0 6.18 1 a ee mz>__ 102030 4050607080 90100 110120130 | Abundance ‘#4732: N-Acetyipyrrolidone 720 7.40 7.60 "7.80 8.00 m/z 82.8, 5.808 | 5000. 7 99 127 30 56 gg 86 2 mz> 10 20.30. 40.5060 _70 8090100. 110 120 130 | 7.20. 7.40 7.60 _ 7.80 8.00 31340.D GCMS0103.M Tue Feb 05 16:53:39 2002 Page 2 NYC-WTC_000017034

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NYC-WTC_000017034Source: NYC Law Department, mirrored locally

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