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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document LSC Area Percent Report ‘pata File : c:\HPCHEM\1\DATA\JANO802\31024.D Vial: 16 Acq On : 9 Jan 2002 3:58 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator! Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.462 260 263 296 rBV 311872 995722 14.95% 2.509% 2 10,996 643 648 658 rBV 150944 350951 5.27% 0.884% 3 11.529 701 706 727 rBV 1944574 5104378 76.63% 12.859% 4 14.163 988 993 1001 rvB 492495 999576 15.01% 2.518% 5 15.118 1092 1097 1117 rBV 3044905 6335848 95.12% 15.962% 6 17,303 1326 1335 1344 rBV2 743156 1508803 22.65% 3.801% 7 18,010 1406 1412 1416 rBv 54849 108150 1.62% 0.272% 8 20.131 1637 1643 1650 rvB 507107 1031002 15.48% 2.597% 9 20.388 1665 1671 1687 rBV 3052287 6579967 98.78% 16.577% 10 20.571 1687 1691 1700 rvB 30810 67180 1.01% 0.169% 11 20.856 1716 1722 1731 rBV 176740 376722 5.66% 0.949% 12 22.637 1910 1916 1924 rBV 328016 632240 9.49% 1.593% 13 24.803 2146 2152 2164 rBV2 3056586 6660990 100.00% 16.781% 14 26.731 2356 2362 2369 rBV 128658 254034 3.81% 0.640% 15 28.503 2548 2555 2561 rBV 84801 177075 2.66% 0.446% 16 29.880 2700 2705 2715 rBV 334533 669396 10.05% 1.686% 17 30.091 2722 2728 2737 rvB 71846 156105 2.348 0.393% 18 31.560 2883 2888 2896 rvB 52262 120350 1.81% 0.303% 19 32.836 3020 3027 3034 rBV2 1898478 4315636 64.79% 10.872% 20 32.928 3034 3037 3048 rvB 55402 158349 2.38% 0.399% 21 34.222 3173 3178 3187 rBV 28068 73107 1.108 0.184% 22 36.903 3463 3470 3491 rBV2 1107361 3018006 45.31% 7.603% Sum of corrected areas: 39693587 31024.D GCMS0103.M Wed Jan 09 12:14:30 2002 NYC-WTC_000017499

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NYC-WTC_000017499Source: NYC Law Department, mirrored locally

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NYC-WTC_000017344

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