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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document 4 ‘S Quantitation Report (QT Reviewed) Wet .t "Data File : C:\HPCHEM\1\DATA\JANO802\31024.D Vial: 16 Acq On : 9 Jan 2002 3:58 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 4:46 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator] Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min: 1) 1,4-Dichlorobenzene-d4 11.53 152 805014 20.00 ug/l 0.00 10) Naphthalene-d8 15.12 136 3102276 20.00 ug/1 0.00 17) Acenaphthene-d10 20.39 164 1501046 20.00 ug/1 0.00 29) Phenanthrene-d10 24.80 188 2205300 20.00 ug/1 0.00 38) Chrysene-d12 32.84 240 1351420 20.00 ug/l 0.00 44) Perylene-d12 36.90 264 801738 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 29.89 235 104905 4.14 ug/mL -0.18 Spiked Amount 5.000 Recovery = 82.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0) N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 to) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.18 128 893 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 0.00 162 to) N.D. 20) Dimethylphthalate 20.13 163 621 N.D. 21) 2,6-Dinitrotoluene 20.12 165 282 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.49 153 187 N.D. 24) 2,4-Dinitrotoluene 20.86 165 1625 N.D. 25) Diethylphthalate 21.91 149 1690 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 fo) N.D. 27) Fluorene 0.00 166 C) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31024.D GCMS0103.M Wed Jan 09 11:57:57 2002 Page 1 NYC-WTC_000017496

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