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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document . . LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 + Acq On : 9 dan 2002 2:59 am Operator: 209 GALOS sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC. peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.465 260 264 277 rBV 355523 990511 15.98% 2.709% 2 7.602 277 279 299 rvB 47473 197887 3.19% 0.541% 3 10.999 644 649 661 rVB 225294 534963 8.63% 1.463% 4 11.522 701 706 727 rBV 1791310 4697405 75.78% 12.847% 5 14.166 989 994 1000 rvB 474876 902944 14.57% 2.469% 6 15,121 1093 1098 1117 rBV 2839871 5844580 94.29% 15,984% 7 15.736 1159 1165 1171 rBV2 29041 71610 1.16% 0.196% 8 17.306 1326 1336 1345 rBV 615940 1199691 19.35% 3.281% 9 18.004 1408 1412 1419 rvB 45874 83530 1.35% 0.228% 10 20.124 1638 1643 1651 rBV 398719 766061 12.36% 2.095% 11 20.391 1666 1672 1691 rBV 2998683 6195999 99.95% 16.945% 12 20.850 1718 1722 1733 rBV 161405 324311 5.23% 0.887% 13 22.640 1911 1917 1923 rBV 223365 439329 7.09% 1.202% 14 24,806 2147 2153 2166 rBV2 2896559 6198797 100.00% 16.953% 15 26.734 2356 2363 2368 rBV 88026 171296 2.76% 0.468% 16 28.497 2550 2555 2560 rvB 58652 117521 1.90% 0.321% 17 29.883 2701 2706 2714 rBV 329255 663674 10.71% 1.815% 18 30.094 2723 2729 2735 rBV 46558 96523 1.56% 0.264% 19 31.563 2884 2889 2893 rBV 31772 70213 «1.13% 0.192% 20 32.839 3021 3028 3035 rBV2 1745944 4119678 66.46% 11.267% 21 32.931 3035 3038 3048 rvB 37161 102679 1.66% 0.281% 22 33.133 3055 3060 3070 rvB 50615 118639 1.918 0.324% 23 36.897 3464 3470 3486 rBV2 986901 2657117 42.87% 7.267% Sum of corrected areas: 36564958 31020.D GCMS0103.M Wed Jan 09 12:11:08 2002 NYC-WTC_000017464

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NYC-WTC_000017464Source: NYC Law Department, mirrored locally

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