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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document : q Quantitation Report (QT Reviewed) ¢ WPata File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:17 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. QIon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.52 152 732250 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 2859197 20.00 ug/L 0.00 17) Acenaphthene-d10 20.39 164 1397076 20.00 ug/1 0.00 29) Phenanthrene-di0 24.81 188 2093398 20.00 ug/l 0.00 38) Chrysene-di2 32.84 240 1281194 20.00 ug/l 0.00 44) Perylene-d12 36.90 264 715973 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 29.88 235 104800 4.36 ug/ml -0.19 Spiked Amount 5.000 Recovery = 87.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.16 74 225 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0) N.D. 4) 1,3-Dichlorobenzene 0.00 146 ° N.D. 5) 1,4-Dichlorobenzene 0.00 146 ° N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 13.299 77 113 N.D. 12) Isophorone 13.89 82 196 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. { 15) Naphthalene 15.19 128 1689 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 18.68 162 200 N.D. 20) Dimethylphthalate 19.79 163 229 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 19,93 152 346 N.D. 23) Acenaphthene 20.47 153 664 N.D. 24) 2,4-Dinitrotoluene 20.85 165 1202 N.D. 25) Diethylphthalate 21.91 149 1092 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 ° N.D. 27) Fluorene 22.02 166 451 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31020.D GCMS0103.M Wed Jan 09 11:57:19 2002 Page 1 NYC-WTC_000017461

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