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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Ley LSC Area Percent Report +! Peta File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.232 126 129 137 rBV 32374 84098 1.23% 0.193% 2 7.463 259 263 296 rVB 333387 1084216 15.80% 2.485% 3 10.997 642 648 656 rBV 232495 532290 7.76% 1.220% 4 11.529 701 706 729 rBV 1792992 4980999 72.59% 11.415% 5 14.164 988 993 1001 rVB 755605 1523860 22.21% 3.492% 6 15.119 1092 1097 1110 rBV 3005589 6197978 90.32% 14.204% 7° (15.734 1159 1164 1175 rBV 39230 100296 1.46% 0.230% 8 17.304 1324 1335 1344 rBV 1110895 2290575 33.38% 5.249% 9 18,002 1406 1411 1416 rBV 83885 153033 2.23% 0.351% 10 20.122 1637 1642 1651 rBV 778296 1564888 22.81% 3.586% 11 20.388 1665 1671 1685 rBV 3133154 6541681 95.33% 14.991% 12 20.847 1714 1721 1733 rBV 233426 497744 7.25% 1.141% 13 22.638 1910 1916 1925 rvB 508354 985113 14.36% 2.258% 14 24.804 2146 2152 2165 rBV2 3206883 6861892 100.00% 15.725% 15 26.732 2356 2362 2368 rBV 221195 439680 6.41% 1.008% 16 28.495 2549 2554 2561 rBV 158142 334391 4.87% 0.766% 17 29.881 2700 2705 2711 rBV 347444 689902 10.05% 1.581% 18 30.092 2722 2728 2735 rBV 136729 283371 4.13% 0.649% 19 31.561 2881 2888 2896 rBV 102591 228297 3.33% 0.523% 20 32.837 3020 3027 3033 rBV2 1869252 4365845 63.62% 10.005% 21 32.929 3033 3037 3048 rvB2 95945 270222 3.94% 0.619% 22 34.223 3171 3178 3186 rBV 57176 154362 2.25% 0.354% 23 35.417 3301 3308 3321 rBV2 151606 432663 6.31% 0.992% 24 36.555 3425 3432 3441 rBV 22525, 75725 1.108 0.174% 25 36.904 3463 3470 3490 rBV 1106029 2962858 43.18% 6.790% Sum of corrected areas: 43635979 NYC-WTC_000017439

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NYC-WTC_000017439Source: NYC Law Department, mirrored locally

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