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GCMS analysis results for sample AD31018, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017380–000017404

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report tk Sata File C: \HPCHEM\ 1 \DATA\JANO 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.468 260 264 276 rBV 331460 925281 14.51% 2.320% 2 10.993 643 648 658 rVB 313583 731576 11.47% 1.834% 3 11.526 701 706 730 rBV 1735713 4552844 71.38% 11.416% 4 14.170 989 994 1000 rVB 734776 1434106 22.48% 3.596% 5 15.124 1092 1098 1116 rBV 2733598 5704274 89.44% 14.303%

6 15.730 1160 1164 1171 rBV 33592 85382 1.34% 0.214% 7 17.309 1325 1336 1344 rBV 1044878 2062159 32.33% 5.171% 8 18.007 1407 1412 1420 rBV 134790 251046 3.94% 0.629% 9 20.128 1637 1643 1651 rVB 726241 1428679 22.40% 3.582% 10 20.394 1665 1672 1689 rBV 2796449 6021417 94.41% 15.099%

11 20.853 1717 1722 1733 rBV 213913 416534 6.53% 1.044% 12 22.634 1911 1916 1923 rBV 450463 912033 14.30% 2.287% 13 24.810 2146 2153 2164 rBV2 2863755 6378102 100.00% 15.993% 14 26.738 2354 2363 2368 rBV 204418 422534 6.62% 1.060% 15 28.500 2548 2555 2561 rBV 155549 315273 4.94% 0.791%

16 29.886 2700 2706 2716 rVB 337954 674071 10.57% 1.690% 17 30.098 2721 2729 2734 rBV 122344 273270 4.28% 0.685% 18 31.557 2882 2888 2895 rBV 96952 217271 3.41% 0.545% 19 32.833 3021 3027 3034 rBV2 1743169 3908099 61.27% 9.800% 20 32.934 3034 3038 3049 rVB 92798 258212 4.05% 0.647%

21 34.219 3172 3178 3189 rBV 56795 146376 2.29% 0.367% 22 35.422 3302 3309 3320 rBV 36287 104543 1.64% 0.262% 23 36.551 3427 3432 3445 rBV3 21367 65695 1.03% 0.165% 24 36.900 3463 3470 3494 rBV2 955524 2524716 39.58% 6.331% 25 39.930 3798 3800 3802 rBV 119471 67016 1.05% 0.168%

Sum of corrected areas: 39880509

NYC-WTC_000017385

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NYC-WTC_000017385Source: NYC Law Department, mirrored locally

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