GCMS analysis results for sample AD30607, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.62 2.97 ug/1 922486 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethyl formami de 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 (Abundance Scan 280 (7.617 min): 30607.D (-) m/z 73.00 100.00% i 73

5000 43 7.20 7.40 7.60 7.80 8.00 • ■ । ■ ■ ■ ■ । * ■ ■ • । ■ ,38,11,1,50,-5524,60, +67+ , 1 l tr 87 103 18 ’rt ■ | ■ । m/z 43.00 32.67% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 I ' ■ ‘ 1 I ‘ 1 ‘ ■ i • ■ TTuur 7.20 7.40 7.60 7.130 8.00 55 m/z 45.0,5 11.57% 27 45 87 ,1, ,! ■ ■ i ■ ■ • ' । • ■ • ■ । • 39I" • ' * i > • 1-‘ 1***1* l■ ■ i ■ l । । j .. miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 TTTITIttriasiyu -TT । 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.0,0 11.26% 44 58

...25. ■ । ■ ■ ■ ■ । • 1 । ■ • ■ ■ । ■ 1 ■ • i ■ ■ ■ • । • ■ ■ • । ■ ■ ■ • । ■ 1 m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.46% 5000 45

........... 27 33 39, 55 ’*I**’I’’*I** ‘i 1 • • 1 I l ss" 1 1 I > 1'1 * • • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' • —1nnmmn—tuTDPrrem m/z~> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30607.D GCMS0103.M Thu Jan 10 14:55:31 2002 Page 1

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