GCMS chemical analysis results, Jan 2002

NYC 9/11 Public Portal Document . Quantitation Report (QT Reviewed) + Data File : C:\HPCHEM\1\DATA\DEC2101\REFE.D Vial: 16 “Acq on : 22 Dec 2001 11:24 pm Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 23 0:13 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min 1) 1,4-Dichlorobenzene-d4 11.67 152 818273 20.00 ug/l -0.03 10) Naphthalene-d8 15.28 136 3147977 20.00 ug/l -0.03 17) Acenaphthene-d1o 20.56 164 1552904 20.00 ug/l -0.02 29) Phenanthrene-d10 24.97 188 2133135 20.00 ug/l -0.02 38) Chrysene-di2 33.01 240 1184379 20.00 ug/l -0.02 44) Perylene-di2 37.10 264 775928 20.00 ug/l -0.02 System Monitoring Compounds 37) 2,4-DDD 30.06 235 100994 3.27 ug/mb -0.01 Spiked Amount 5.000 Recovery = 65.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.42 74 65104 1.81 ug/1 84 3) bis (2-Chloroethyl) ether 11.10 93 165116 2.92 ug/1 91 4) 1,3-Dichlorobenzene 11.58 146 100159 1.68 ug/l 96 5) 1,4-Dichlorobenzene 11.58 146 100159 1.66 ug/l 96 6) 1,2-Dichlorobenzene 12.23 146 114086 2.06 ug/l 99 7) 2,2'-oxybis(1-Chloropropan 12.57 45 280444 3.90 ug/l # 90 8) N-Nitroso-di-n-propylamine 12.96 70 112306 3.49 ug/1 93 9) Hexachloroethane 13.06 117 27582 1.26 ug/l 97 11) Nitrobenzene 13.37 77 144915 2.95 ug/l # 86 12) Isophorone 14.00 82 316715 3.35 ug/l 93 13) bis(2-Chloroethoxy)methane 14.70 93 185974 2.93 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 96723 2.12 ug/l 96 15) Naphthalene 15.33 128 422897 2.81 ug/l 99 16) Hexachlorobutadiene 15.88 225 24577 1.10 ug/1 97 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 18.84 162 225396 2.54 ug/l 95 20) Dimethylphthalate 19.94 163 312835 3.03 ug/1 100 21) 2,6-Dinitrotoluene 20.15 165 46411 1.90 ug/l # 59 22) Acenaphthylene 20.09 152 343474 2.76 ug/1 99 23) Acenaphthene 20.64 153 265385 2.98 ug/l 100 24) 2,4-Dinitrotoluene 21.34 165 46931 1.51 ug/l # 74 25) Diethylphthalate 22.06 149 324998 3.40 ug/1 98 26) 4-Chlorophenyl-phenylether 22.20 204 125504 3.01 ug/l 95 27) Fluorene 22.16 166 271923 2.98 ug/l 98 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 305897 3.10 ug/L # 90 (#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Thu Dec 27 09:44:32 2001 Page 1 NYC-WTC_000017141