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GCMS analysis results for sample AD30601, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.

NYC-WTC_000017126–000017138

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 11 10:40 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.04 178 1182 N.D. 34) Anthracene 25.18 178 191 N.D. 35) Di-n-butylphthalate 27.04 149 16726 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 29.47 202 191 N.D. 40) Butylbenzylphthalate 31.53 149 304 N.D. 41) Benzo(a)anthracene 33.03 228 6502 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 7445 N.D. 43) Chrysene 33.09 228 2274 N.D. 45) Di-n-Octylphthalate 35.04 149 407 N.D. 46) Benzo(b)fluoranthene 36.10 252 2841 N.D. 47) Benzo(k)fluoranthene 36.10 252 1050 N.D. 48) Benzo(a)pyrene 36.98 252 528 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz (a,h) anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D GCMS0103.M Fri Jan 11 10:40:32 2002 Page 2

NYC-WTC_000017128

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NYC-WTC_000017128Source: NYC Law Department, mirrored locally

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