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GCMS analysis results for sample AD30607, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.

NYC-WTC_000017171–000017191

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 9:02 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.04 178 1198 N.D. 34) Anthracene 25.04 178 1198 N.D. 35) Di-n-butylphthalate 27.03 149 5141 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.72 149 1998 N.D. 41) Benzo(a)anthracene 33.03 228 4722 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 8816 N.D. 43) Chrysene 33.03 228 4722 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.11 252 4389 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30607.D GCMS0103.M Tue Jan 15 09:03:25 2002 Page 2

NYC-WTC_000017174

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NYC-WTC_000017174Source: NYC Law Department, mirrored locally

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