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GCMS analysis results for sample AD30601, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.

NYC-WTC_000017126–000017138

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 11 10:40 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.68 152 1207320 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 4653884 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 2289224 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.98 188 3443644 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 2020637m 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 1211049 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 168401 3.38 ug/mL 0.00 Spiked Amount 5.000 Recovery = 67.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.34 77 183 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 2084 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.66 153 199 N.D. 24) 2,4-Dinitrotoluene 21.30 165 100 N.D. 25) Diethylphthalate 22.18 149 985 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D GCMS0103.M Fri Jan 11 10:40:28 2002 Page 1

NYC-WTC_000017127

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