GCMS analysis of environmental sample AD30087 conducted January 9, 2002.
NYC-WTC_000016737–000016745Folder label: “GCMS X 12/12/01 A 12/19/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1901\30087.D Vial: 14 Acq On : 20 Dec 2001 2:08 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 15:56 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update ‘: Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.68 152 881445 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3405107 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1691766 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2451950m 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1635648 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1046440 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.06 235 134689 3.80 ug/mL -0.01 Spiked Amount 5.000 Recovery = 76.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachioroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 709 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyc1opentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.13 165 197 N.D. 25) Diethylphthalate 22.12 149 215 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30087.D GCMS1126.M Thu Jan 03 10:18:55 2002 Page 1
NYC-WTC_000016739
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NYC-WTC_000019081
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30260 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016699
GCMS analysis of environmental sample AD30021 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019061
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30085 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016746
GCMS analysis of environmental sample AD30086 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016854
Laboratory report documenting GCMS analysis of environmental sample AD30109 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016717
GCMS analysis of environmental sample AD30113 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016708
Gas chromatography-mass spectrometry analysis of sample AD30022 conducted January 9, 2002, measuring organic compounds with 80% surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019121
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30314 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019090
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30254 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019153
Gas chromatography-mass spectrometry analysis report for sample AD30255, completed January 9, 2002, showing 2,4-DDD surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035683
Laboratory notes stating the GCMS scan of sample AD28898 revealed no unusual compounds.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035598
Lab report noting no unusual compounds but recovery issues and low pH in a water sample.
1 shared topics · similarity 0.998
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NYC-WTC_000016680
Document header or index page associated with gas chromatography mass spectrometry records from December 2001.
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NYC-WTC_000016681
Method blank report confirming absence of contamination during volatile organic compound testing procedures in January 2002.
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GCMS calibration report listing target compounds and response factors for December 2001 analysis.
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NYC-WTC_000016694
Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.
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NYC-WTC_000016699
GCMS analysis of environmental sample AD30021 conducted January 9, 2002.
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