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GCMS unknowns analysis report for sample AD31342, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31342 using GCMS on February 11, 2002.

NYC-WTC_000017004–000017015

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017012
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0902\31342.D Vial: 8 Acq On : 10 Jan 2002 10:23 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE FIDE SIS ISS ISIS EISEI ISIS ISIS ISIS ISIS ICIS IOS GSCI IOI ITO IIE Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.61 0.84 ug/1 158083 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 2-Propanghe, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 64 2 1-Fluorgénonane 146 COH19F 000463-18-3 12 3 Reet acid, sec-octyl ester 172 C10H2002 054515-77-4 9 _4 Decane, 1-fluoro- — 160 ClOH21F ——s———(000334-56-5 9 Abundance Scan 278 (7.608 min}: 313420 Cy " 43.05 100.00 53 61 83 97 447125 7.20__740 7.60 _7.80__8.00 r Hp | m/z-124.8 9.16! mz->____10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170. __ AbUnCaRSS 2BAT: Z-Propanone, 1.1,1-Wichloro- 7 i. | [120 "740 "7.60 "7.80 8.00 45 m/z 82.8 7.68 38 8597 447128 miz-> ___10_ 20 30.40 50 60 70 80 90 100 110 120 130 140 150 160.170 | ‘Abundances cs ET 4&3 7207.40 7.60 7.80 _ 8.00 5000. m/z 83.8, 7.60: Fd 8 a0 H 84 97 wy fnlz->_10_20. 30 4050 6070 8090 100 110 120 130 140 150 160 170. | ‘Abundances #1771 Acelié acid, sec-octyl estar poe ee eB 7.20 740 7.60 7.80 8.00 [m/z 81.9 6.76) | 5000: or | . 70 112 | miz> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 7.20. 7.40 7.80. 7.80 8,00. 31342.D GCMS0103.M Tue Feb 05 16:55:10 2002 Page 2 NYC-WTC_000017012

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NYC-WTC_000017012Source: NYC Law Department, mirrored locally

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