GCMS analysis results for sample AD31345, Feb 2002

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Data File : C: \HPCHEM\ 1 \DATA\JANO 90231345.D Vial: 11 Acq On : 11 Jan 2002 1:19 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.60 0.68 ug/1 132176 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Propanone/ 1,1,1 - trichloro- 160 C3H3C130 000918-00-3 38 2 1-Fluorononane 146 C9H19F 000463-18-3 9 3 4-Penten-2-one 84 C5H80 013891-87-7 4 4 2-Acetyl-l,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 Abundance Scan 279 (7.603 min): 31345.D (-) m/z 4 ’.05 100.00% 43

5000

37 ++ ,49 63 72 8288 thpri i 'J' ' । 111 i । i । 141 । । । 1 ! 119125 97 7.20 7.40 7.60 7.80 8.00 ■ ■ i ‘ • i ■ ■ ■ ■ i • i ii m/z 124.85 10.33% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 nB—mnC—nnNn 7.20 7.40 7.60 7.80 8.00 15 m/z 96.95 8.90% 35 49 85 97 117 I?? ■ ■ i 1 ■ ■ • i • • • ■ i ■ ■ i ■ ■ ■ ' i ‘ —TIO-Fuuposmuuuiriru • 1 i • ■ • ■ i • ■ ■ ■ i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8922: 1-Fjucrononane 43 ■ i * • • < । * - 7.20 7.40 7.60 7.80 8.00 5000 m/z 81.9, 7.37% 56 27 70 i 84 97 : 33 I Hi ■ ■ i ■ ■ ■ • i • • ■ • i' ‘ ■ i' •1 • i ■ ■ ■ ■ i ■ ■' ■ i ■ 11 ■ ■ ■' । ■ ■ ■ ■ । ■ ■ ■' । ■ ■ ■ ■ । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #555:4-Penten-2-one ' i ‘ ‘ i 1 ' 1 ' 1 1 1 1 ' I ' ' 1 1 1 1 1 43 7.20 7.40 7.60 7.80 8.00 m/ z 84.85 6.75%

5000

15 1 T—mT27 37, fr *14*4614*481* 53 69 84 1G m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.20 7.40 7.60 7.80 8.00

31345.D GCMS0103.M Tue Feb 05 16:57:35 2002 Page 2

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