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GCMS blank analysis results for sample AD31249, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting a GCMS blank analysis for sample AD31249 conducted on January 29, 2002.

NYC-WTC_000016921–000016928

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016925
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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\JAN0902\LB.D Vial: 4 Acq On : 10 Jan 2002 6:27 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.465 260 264 286 rBV 304265 882485 15.18% 3.026% 2 11.523 702 706 726 rBV 1606312 4348639 74.79% 14.910% 3 15.121 1093 1098 1118 rBV 2686797 5549700 95.45% 19.028% 4 20.391 1666 1672 1691 rBV 2877321 5814487 100.00% 19.936% 5 24.806 2147 2153 2165 rBV2 2595316 5576553 95.91% 19.120%

6 29.883 2701 2706 2714 rBV 373701 734051 12.62% 2.517% 7 32.839 3021 3028 3047 rBV 1589674 3789044 65.17% 12.991% 8 36.906 3464 3471 3485 rBV2 865075 2470807 42.49% 8.472%

Sum of corrected areas: 29165766

LB.D GCMS0103.M Tue Feb 05 16:59:00 2002

NYC-WTC_000016925

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NYC-WTC_000016925Source: NYC Law Department, mirrored locally

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