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GCMS analysis results for sample AD31133, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31133 performed on February 11, 2002, including detection of unknown compounds.

NYC-WTC_000018994–000019003

Folder label: “GCMS X 12/21/01 A 1/10/02

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Scanned page image, NYC-WTC_000018999
OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\JAN0902\31133.D Vial: 23 Acq On : 10 Jan 2002 12:34 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.471 260 264 271 rBV 258085 681051 9.86% 1.856% 2 7.563 271 274 306 rVB 812579 2432592 35.22% 6.630% 3 11.529 701 706 725 rBV 1981404 5199250 75.28% 14.170% 4 15.127 1092 1098 1116 rBV 3122997 6683833 96.78% 18.216% 5 20.388 1665 1671 1689 rBV 3229137 6906292 100.00% 18.823%

6 24.803 2146 2152 2165 rBV2 2917050 6555028 94.91% 17.865% 7 29.889 2700 2706 2713 rBV 306168 630237 9.13% 1.718% 8 32.836 3021 3027 3051 rBV2 1971550 4530395 65.60% 12.347% 9 36.903 3463 3470 3489 rBV 1098660 3072452 44.49% 8.374%

Sum of corrected areas: 36691130

31133.D GCMS0103.M Wed Feb 06 09:23:22 2002

NYC-WTC_000018999

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NYC-WTC_000018999Source: NYC Law Department, mirrored locally

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