GCMS analysis results for sample AD30116, Jan 2002

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LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC3101\30116.D Vial: 58 Acq On 2 Jan 2002 10:10 pm Operator: 209 GALOS Sample gems scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF' Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.396 143 147 158 rBV5 16080 65929 1.09% 0.222% 2 7.608 275 279 312 rBV 255479 938498 15.50% 3.163% 3 11.675 717 722 740 rBV 1562206 4572070 75.53% 15.411% 4 15.283 1109 1115 1156 rBV 1886134 5865439 96.89% 19.770% 5 20.561 1684 1690 1703 rBV 2139510 6053604 100.00% 20.404%

6 24.986 2166 2172 2216 rBV2 1471572 5727862 94.62% 19.306% 7 30.072 2720 2726 2745 rBV 231034 574981 9.50% 1.938% 8 33.028 3041 3048 3075 rBV2 1087854 3711707 61.31% 12.511% 9 37.123 3487 3494 3519 rBV 485051 2158151 35.65% 7.274%'

Sum of corrected areas: 29668241

30116.D GCMS1126.M Thu Jan 03 10:30:36 2002

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