NYC-WTC_000017913
Laboratory report documenting GCMS analysis of sample AD30490 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
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GCMS analysis results for sample AD30116, Jan 2002
Machine-extracted title · confidence 50%GCMS analysis of environmental sample AD30116 conducted January 9, 2002.
NYC-WTC_000016755–000016763Folder label: “GCMS X 12/12/01 A 12/19/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) 4 •3
Data File C:\HPCHEM\1\DATA\DEC3101\30116.D Vial: 58 Acq On 2 Jan 2002 10:10 pm Operator: 209 GALOS Sample gems scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 9:56 2002 Quant Results File: GCMS1126.RES
Quant Method-: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 748525 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 2855729 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 1418910 20.00 ug/1 -0.01 2 9) Phenanthrene-dl0 24.99 188 1999579m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1158459 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 604431 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 91343 4.16 ug/mL 0.00 Spiked Amount 5.000 Recovery = 83.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.31 74 102 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichiorobenzene 0.00 146 0 N.D. 6) 1,2-Dichiorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.14 77 100 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.36 128 748 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.06 165 425 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30116.D GCMS1126.M Thu Jan 03 09:56:40 2002 Page 1
NYC-WTC_000016757
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NYC-WTC_000016757Source: NYC Law Department, mirrored locally
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