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GCMS reference analysis results, Jan-Feb 2002

Machine-extracted title · confidence 100%

Analytical results for volatile organic compounds including nitrosamines and chlorinated benzenes.

NYC-WTC_000016370–000016374

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JANO 8 02\REFC.D Vial: 5 Acq On 9 Jan 2002 5:39 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 10:55 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.43 168 76597 2.09 ug/1 96 31) 4-Bromophenyl-phenylether 23.49 248 44700 2.15 ug/1 95 32) Hexachlorobenzene 23.91 284 53816 2.23 ug/1 99 3 3) Phenanthrene 24.87 178 278584 2.46 ug/1 99 34) Anthracene 25.01 178 250646 2.26 ug/1 99 35) Di-n-butylphthalate 26.83 149 372559 2.43 ug/1 99 36) Fluoranthene 28.48 202 263289 2.42 ug/1 99 39) Pyrene 29.15 202 276672 2.25 ug/1 98 40) Butylbenzylphthalate 31.33 149 114102 1.71 ug/1 96 41) Benzo(a)anthracene 32.78 228 181987 2.35 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.14 149 144943 1.61 ug/1 99 43) Chrysene 32.91 228 199351 2.62 ug/1 98 45) Di-n-Octylphthalate 34.88 149 129136 1.01 ug/1 # 96 46) Benzo(b)fluoranthene 35.87 252 122265 1.85 ug/1 97 47) Benzo(k)fluoranthene 35.92 252 167424 2.58 ug/1 97 48) Benzo(a)pyrene 36.74 252 94544 1.83 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.50 276 88128 1.80 ug/1 99 5 0) Dibenz(a,h)anthracene 40.55 278 77232 2.06 ug/1 99 51) Benzo(g,h,i)perylene 41.54 276 85522 2.10 ug/1 94

(#) = qualifier out of range (m) = manual integration REFC.D GCMS0103.M Wed Feb 06 10:57:22 2002 Page 2

NYC-WTC_0000 16373

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NYC-WTC_000016373Source: NYC Law Department, mirrored locally

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