GCMS calibration table review, Jan 17, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\JAN1602\31460.D Vial: 23 Acq On : 17 Jan 2002 9:08 am Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Miso Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 11:55 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) . Title : 209 625/TCLP calibration table 0 Last Update : Mon Jan 07 10:31:02 2002 ( . . J Response via : Initial Calibration L 2 MA DataAcq Meth : GCMS0103 /) 0/

Internal Standards R.T. Qlon Response Cone Units Dey(Min)

1) 1,4-Dichiorobenzene -d4 11.50 152 797634 20.00 ug/1 -0.03 10) Naphthalene-d8 15.10 136 3085775 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.36 164 1.560031 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 2161432 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1411952 20.00 ug/1 -0.04 44) Perylene-dl2 36.86 264 959064 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 29.85 235 78205 3.15 ug/mL -0.22 Spiked Amount 5.000 Recove: = 63.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.16 128 884 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.78 165 467 N.D. 25) Diethylphthalate 21.89 149 859 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31460.D GCMS0103.M Thu Feb 07 11:55:51 2002 Page 1

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