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GCMS calibration table review, Jan 17, 2002

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Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 17, 2002.

NYC-WTC_000016352–000016358

Folder label: “GCMS X 12/28/01 A 1/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1602\31460.D Vial: 23 Acq On : 17 Jan 2002 9:08 am Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 11:55 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine • 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.84 178 185 N.D. 34) Anthracene 24.84 178 185 N.D. 35) Di-n-butylphthalate 26.80 149 6680 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.80 228 3591 N.D. 42) Bis(2-ethylhexyl)phthalate 33.11 149 3689 N.D. 43) Chrysene 32.80 228 3591 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 36.86 252 3702 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31460.D GCMS0103.M Thu Feb 07 11:55:55 2002 Page 2

NYC-WTC_000016353

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NYC-WTC_000016353Source: NYC Law Department, mirrored locally

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