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GCMS analysis summary, sample AD31376, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31376 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016169–000016177

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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Scanned page image, NYC-WTC_000016174
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31376.D Vial: 20 Acq On : 16 Jan 2002 5:33 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0 .2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.456 259 263 282 rBV 160722 479848 7.86% 1.613% 2 11.496 698 703 722 rBV 1780859 4602106 75.41% 15.467% 3 15.094 1089 1095 1114 rBV 2832803 5909990 96.85% 19.862% 4 20.355 1661 1668 1686 rBV 2972298 6102463 100.00% 20.509% 5 24.770 2143 2149 2162 rBV2 2648464 5664315 92.82% 19.037%

6 29.847 2697 2702 2709 rBV2 294513 570180 9.34% 1.916% 7 32.794 3017 3023 3043 rBV2 1501997 3673538 60.20% 12.346% 8 36.861 3460 3466 3486 rBV2 984756 2752289 45.10% 9.250%

Sum of corrected areas: 29754729

31376.D GCMS1126.M Mon Feb 04 15:06:26 2002

NYC-WTC_000016174

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NYC-WTC_000016174Source: NYC Law Department, mirrored locally

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