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GCMS analysis summary, sample AD31349, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31349 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016178–000016186

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31349.D Vial: 24 Acq On : 16 Jan 2002 10:26 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.446 258 262 294 rBV 404567 1090733 17.97% 3.500% 2 11.494 698 703 724 rBV 1729807 4586199 75.57% 14.715% 3 15.093 1089 1095 1113 rBV 2823133 5863799 96.62% 18.814% 4 20.353 1661 1668 1685 rBV 2895854 6068786 100.00% 19.472% 5 24.769 2142 2149 2162 rBV2 2612330 5654964 93.18% 18.144%

6 29.855 2697 2703 2711 rBV 419521 864104 14.24% 2.772% 7 32.802 3018 3024 3044 rBV 1742508 4027724 66.37% 12.923% 8 36.869 3459 3467 3484 rBV 1060150 3011143 49.62% 9.661%

Sum of corrected areas: 31167452

31349.D GCMS1126.M Mon Feb 04 15:03:25 2002

NYC-WTC_000016183

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NYC-WTC_000016183Source: NYC Law Department, mirrored locally

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