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GCMS analysis summary, sample AD31374, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31374 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016149–000016158

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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Scanned page image, NYC-WTC_000016154
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31374.D Vial: 19 Acq On : 16 Jan 2002 4:34 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.446 258 262 293 rVB 326663 962621 15.66% 3.228% 2 11.504 699 704 724 rBV 1788219 4756230 77.38% 15.950% 3 14.139 987 991 997 rVB 50026 101026 1.64% 0.339% 4 15.094 1090 1095 1114 rBV 2906669 5962112 97.00% 19.993% 5 20.354 1662 1668 1683 rBV 2909650 6146509 100.00% 20.612%

6 24.770 2143 2149 2161 rBV2 2592927 5548439 90.27% 18.606% 7 29.846 2697 2702 2710 rBV 378638 776004 12.63% 2.602% 8 32.793 3017 3023 3044 rBV2 1377414 3280318 53.37% 11.000% 9 36.860 3460 3466 3490 rBV 811976 2287109 37.21% 7.670%

Sum of corrected areas: 29820368

31374.D GCMS1126.M Mon Feb 04 15:04:50 2002

NYC-WTC_000016154

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NYC-WTC_000016154Source: NYC Law Department, mirrored locally

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