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GCMS analysis summary, sample AD31381, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31381 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016187–000016194

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\JAN1502\31381.D vial: 14 Acq On : 15 Jan 2002 11:41 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.504 699 704 729 rBV 1613660 4539993 76.31% 15.488% 2 15.093 1090 1095 1114 rBV 2726136 5718095 96.12% 19.507% 3 20.354 1662 1668 1681 rBV 2831208 5949181 100.00% 20.296% 4 24.769 2143 2149 2162 rBV2 2577608 5461691 91.81% 18.633% 5 29.846 2697 2702 2711 rBV 252064 517860 8.70% 1.767%

6 32.802 3017 3024 3048 rBV2 1688155 3959485 66.56% 13.508% 7 36.869 3460 3467 3487 rBV 1123713 3166268 53.22% 10.802%

Sum of corrected areas: 29312573

31381.D GCMS1126.M Mon Feb 04 15:10:12 2002

NYC-WTC_000016192

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NYC-WTC_000016192Source: NYC Law Department, mirrored locally

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