Calibration table for GCMS analysis listing surrogate compounds and response factors from January 16, 2002.
NYC-WTC_000016118–000016124Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JANI502\27288FB.D Vial: 21 Acq On : 16 Jan 2002 6:31 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P. Quant Time: Feb 4 14:41 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.50 152 647080 20.00 ug/1 -0.20 10) Naphthalene-d8 15.09 136 2527855 20.00 ug/1 -0.21 17) Acenaphthene-diO 20.35 164 1258394 20.00 ug/1 -0.22 29) Phenanthrene-diO 24.77 188 1676867 20.00 ug/1 -0.22 38) Chrysene-dl2 32.79 240 948835 20.00 ug/1 -0.24 44) Perylene-dl2 36.86 264 626644 20.00 ug/1 -0.26
System Monitoring Compounds 37) 2,4-DDD 29.85 235 85807 4.65 ug/mL -0.22 Spiked Amount 5.000 Recovery = 93.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.15 128 757 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.69 165 178 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 27288FB.D GCMS1126.M Mon Feb 04 14:42:16 2002 Page 1
NYC-WTC_000016118
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000016352
Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016555
Blank analysis report for DEP sample AD31432 showing non-detect levels for volatile organic compounds from January 22, 2002.
Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009650
Calibration table page listing internal standards and response factors for GCMS analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035737
Laboratory notes stating the GCMS scan of sample AD28862 revealed no unusual compounds.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009670
Laboratory file showing GC/MS calibration response factors for surrogate compounds from February and March 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009686
Laboratory file showing GC/MS calibration response factors for surrogate compounds from February and March 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034741
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.
Similar document embedding; no shared entity or topic indexed. · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058798
Laboratory report page showing surrogate recovery data for sample AE01153 analyzed on March 22, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034790
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28599 analyzed in early December 2001.
Similar document embedding; no shared entity or topic indexed. · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034376
Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034799
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28593 analyzed in early December 2001.
Similar document embedding; no shared entity or topic indexed. · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034877
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28477 analyzed in early December 2001.
Similar document embedding; no shared entity or topic indexed. · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000016055
DEP GCMS analysis log covering samples processed between late December 2001 and mid-January 2002.
Filed in the same folder
NYC-WTC_000016056
Technical log detailing extraction rates, volumes, and pH settings used during sample preparation for GCMS analysis.
Filed in the same folder
NYC-WTC_000016058
Documentation of instrument settings and calibration parameters for Method 508 analysis conducted in early 2002.
Filed in the same folder
NYC-WTC_000016061
Calibration data sheet listing response factors for various organic compounds including nitrosamines and chlorinated benzenes.
Filed in the same folder
NYC-WTC_000016065
Calibration report showing retention times and response factors for deuterated internal standards used in PAH analysis.
Filed in the same folder