Calibration table for GCMS analysis listing surrogate compounds and response factors from January 16, 2002.
NYC-WTC_000016118–000016124Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JANI502\27288FB.D Vial: 21 Acq On : 16 Jan 2002 6:31 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 14:41 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.84 178 199 N.D. 34) Anthracene 24.84 178 199 N.D. 35) Di-n-butylphthalate 26.80 149 7650 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.79 228 2308 N.D. 42) Bis(2-ethylhexyl)phthalate 33.11 149 2117 N.D. 43) Chrysene 32.79 228 2308 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.86 252 2406 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.
(#) = qualifier out of range (m) = manual integration 27288FB.D GCMS1126.M Mon Feb 04 14:42:20 2002 Page 2
NYC-WTC_000016119
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Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 17, 2002.
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Laboratory file showing GC/MS calibration response factors for surrogate compounds from February and March 2002.
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Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28593 analyzed in early December 2001.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28477 analyzed in early December 2001.
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