Pesticide analysis results, sample AE11755, May 2002

NYC 9/11 Public Portal Document Library Search Coinpound Report

Data File : C:\MSDCHEM\1\DATA\051302\LBB0513.D Vial: 12 • Acq On : 13 May 2002 8:50 pm Operator: Bohlk / Inst 213 Sample : LB 5/13/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Tetracosane (CAS) $$ n-Tetr... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.75 0.05 ug/L 43678 Phenanthrene d-10 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 86 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 83 3 Nonadecane $$ n-Nonadecane 268 C19H40 000629-92-5 80 4 Heptadecane 240 C17H36 000629-78-7 72 Abundance Scan 1287 (22.749 min): LBB0513.D (-) m/ z 57.10 100.00% 57

5000 85

113 AAAWA 22.40 22.60 22.80 23.00 m/z 71.10 86.68% 0 0810011113 m/z-> 20 40 60 80 100120140 160180200220240 260280 300 320 340 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane 57

5000 85 nALata 22.40 22.60 22.80 23.00 m/z 85.10 49.27% 113 ,| j 141 169 197 225 253 281 309 338 0- ■ >'t 11 n 111 ■ । i'i 11 h i p । ■ f| 111 n > ■ > r 11 n 11 f 1111 j ■ ■ 111 n 11*| i ■ m/z—> 20 40 60 80 100 120140160 180 200 220 240260280 300 320 340 Abundance #211487: Nonadecane (CAS)$$ n-Nonadecane 433

71 L ’ i ‘ * 22.40 22.60 22.80 23.00 5000 m/z 99.00 20.27%

99 J 127 _ 154 183 268 0 T—ogamg m/z—> 20 40 60 80 100120140160180200220240260280 300 320340 Abundance #211486: Nonadecane $$ n-Nonadecane 57 22.40 22.60 22.80 23.00 m/z 55.10 19.53%

85 5000

29

m/z-> 0TH 4.41134141 169 197 (. r.. । 268 /1.... ।. 141 <. ।. I.. ।.... ।....,.... ।. 20 40 60 80 100 120 140 160 180200 220 240260 280 300320 340 22.40 22.60 22.80 23.00

BB0513.D 050802.M Tue May 14 11:03:07 2002 Page 5

NYC-WTC_000016003