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← Document results/DEP Box 15/508 X 5/10/02 5/14/02
Document / 9 pages

GCMS pesticide analysis report, sample AE10996, May 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for the detection of organochlorine pesticides including Aldrin and Dieldrin.

NYC-WTC_000015854–000015862

Folder label: “508 X 5/10/02 5/14/02

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NYC 9/11 Public Portal Document quantltatlon Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\020514\PESTC1.D\ECD1A.CH Vial: 4 Signal #2 : C:\MSDCHEM\1\DATA\508\020514\PESTC1.D\ECD2B.CH Acq On : 14 May 2002 10:23 am Operator: Nefliu Sample : pest ici Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E Quant Time: May 16 10:46:40 2002 Quant Results File: 020514P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020514P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Tue May 14 13:42:09 2002 Response via : Initial Calibration DataAcq Meth : 508P.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 13.02 13.52 945.1E6 1032.6E6 0.191 0.194 Spiked Amount 0.200 Recovery = 95.50% 97.00%

Target Compounds Propachlor 8.29 7.77 27120130 29850251 0.046 / 0.046 1) 2) g-BHC 8.99 9.29 642.0E6 660.6E6 0.05406 0.057 3) Heptachlor 10.04 10.23 171.3E6 175.5E6 0.018^4 0.019 4) Aldrin 10.68 10.90 267.2E6 296.5E6 0.0239% 0.025 5) Heptachlor Epoxi 11.97 12.11 479.7E6 509.4E6 0.048 100 0.050 6) 4,4-DDE 12.69 13.16 691.8E6 735.4E6 0.07695 0.080 7) Dieldrin 13.20 13.38 218.5E6 188.3E6 0.018 It 3 0.016 8) Endrin 13.62 13.92 260.OE6 283.1E6 0.03793 0.040 9) Methoxychlor 15.14 15.87 200.OE6 175.3E6 0.078 08 0.072m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTCI.D 020514P.M Thu May 16 10:47:07 2002 Page 1

NYC-WTC_000015855

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NYC-WTC_000015855Source: NYC Law Department, mirrored locally

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