NYC Law Department release
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← Document results/DEP Box 15/508 X 5/10/02 5/14/02
Document / 7 pages

GCMS pesticide analysis summary, sample AE10996, May 2002

Machine-extracted title · confidence 95%

Summary of gas chromatography-mass spectrometry results for multiple pesticides showing average concentrations and percent relative standard deviation.

NYC-WTC_000015863–000015869

Folder label: “508 X 5/10/02 5/14/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\020514\PESTC2.D\ECDlA.CH Vial: 5 signal #2 : C:\MSDCHEM\l\DATA\508\020514\PESTC2.D\ECD2B.CH Acq On : 14 May 2002 10:45 am Operator: Nefliu Sample : pest id Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E Quant Time: May 16 10:47:14 2002 Quant Results File: 020514P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020514P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Tue May 14 13:42:09 2002 Response via : Initial Calibration DataAcq Meth : 508P-M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 13.02 13.52 977.7E6 1023.OE6 0.197 0.192 Spiked Amount 0.200 Recovery = 98.50% 96.00%

Target Compounds 1) Propachlor 8.29 7.77 112.6E6 123.3E6 0.189 0.191 2) g-BHC 8.99 9.29 3380.5E6 3249.4E6 0.283 0.279 3) Heptachlor 10.04 10.23 926.1E6 887.1E6 0.097 0.095 4) Aldrin 10.68 10.90 1412.1E6 1432.2E6 0.121 0.119 5) Heptachlor Epoxi 11.97 12.11 2409.1E6 2380.1E6 0.240 0.236 6) 4,4 -DDE 12.69 13.16 3719.7E6 3641.6E6 0.407 0.398 7) Dieldrin 13.20 13.39 905.0E6 904.7E6 0.075 0.079 8) Endrin 13.62 13.93 1455.6E6 1445.OE6 0.208 0.202 9) Methoxychlor 15.14 15.87 1052.0E6 1004.4E6 0.410 0.414

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTC2.D 020514P.M Thu May 16 10:47:23 2002 Page 1

NYC-WTC_000015864

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NYC-WTC_000015864Source: NYC Law Department, mirrored locally

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