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← Document results/DEP Box 68/508 X 11/27/01 A 12/4-12/26/01
Document / 7 pages

Second pesticide calibration verification for sample AD27828, Jan 2002

Machine-extracted title · confidence 90%

Duplicate calibration verification results for pesticides and PCBs confirming analytical system performance.

NYC-WTC_000089583–000089589

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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Scanned page image, NYC-WTC_000089584
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O11226\PESTC1.D\ECD1A.CH Vial: 5 Signal #2 : C:\MSDCHEM\1\DATA\508\011226\PESTCI.D\ECD2 B.CH Acq On : 26 Dec 2001 9:48 am Operator: Nefliu Sample : pest id Inst Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 26 10:46:00 2001 Quant Results File: 011224P.RES Quant Method : C:\MSDCHEM\1\METHODS\011224P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 10:35:07 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 831.2E6 539.5E6 0.214m 0.184 Spiked Amount 0.200 Recovery = 107.00% 92.00%

Target Compounds 1) Propachlor 9.06 8.50 24913369 16158779 0.047m VOV|. 0.043 2) g-BHC 9.83 10.19 528.8E6 320.2E6 0.061m\<fl- 0.052 3) Heptachlor 11.00 11.23 161.9E6 85985897 0 . O2Om^oI'’ 0.018 4) Aldrin 11.70 11.98 228.4E6 154.4E6 0.026m|C^- . 0.024 5) Heptachlor Epoxi.13.14 13.34 408.4E6 268.6E6 0.054m|\y|. 0.04 9 6) 4,4-DDE 13.97 14.55 621.6E6 422.1E6 0.088 wo]. 0.080 7) Dieldrin 14.55 14.81 141.5E6 86838614 • 0.018m ^yj. 0.015m 8) Endrin 15.06 15.47 248.3E6 154.1E6 0.042m 0.037 9) Methoxychlor 17.00 18.02 194.6E6 101.4E6 0.081m .0.074

(f)=RT Delta > 1/2 Window (#)=Amounts differ by 25% (m)=manual int. PESTCI.D 011224P.M Mon Dec 31 11:22:18 2001 Page 1

NYC-WTC_000089584

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NYC-WTC_000089584Source: NYC Law Department, mirrored locally

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