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Pesticide calibration verification results, sample AD31072, Jan 2002

Machine-extracted title · confidence 95%

Calibration data showing recovery percentages for various pesticide standards in sample AD31072.

NYC-WTC_000090524–000090532

Folder label: “508 X 12/21/01 A 1/3/02

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Scanned page image, NYC-WTC_000090525
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\PESTCl.D\ECDlA.CH Vial: 14 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\PESTCl.D\ECD2B.CH Acq On : 03 Jan 2002 8:47 pm Operator: Nefliu Sample : pest id Inst Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 10:52:01 2002 Quant Results File: 020103P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020103P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Jan 04 10:51:09 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.36 14.98 715.0E6 594.5E6 0.193 0.191 SpiJeed Amount 0.2 00 Recovery 96.50% 95.50%

Target Compounds 1) Propachlor 9.06 8.50 23542065 18200877 0.045m 1)3 0.046 2) g-BHC 9.83 10.18 455.3E6 353.9E6 0.056 -(ax’ 0.055 3) Heptachlor 11.00 11.23 140.2E6 99303138 0.019 KK> 0.019 4) Aldrin 11.71 11.98 194.5E6 150.6E6 0.024 too 0.023 5) Heptachlor Epoxi 13.15 13.33 353.9E6 276.1E6 0.050 lioi 0.049 6) 4,4-DDE 13.99 14.54 511.0E6 404.3E6 0.08010^ 0.079 7) Dieldrin 14.57 14.80 123.5E6 97686413 0.017m |0t, 0.015 8) Endrin 15.07 15.46 204.3E6 152.7E6 0.041j<jr 0.039 9) Methoxychlor 17.02 18.01 174.1E6 116.0E6 0.079 0.078

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTCI.D 020103C.M Mon Jan 07 10:56:44 2002 Page 1

NYC-WTC_000090525

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NYC-WTC_000090525Source: NYC Law Department, mirrored locally

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