GCMS surrogate recovery report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\061102\12763.D Vial: 7 Acq On : 11 Jun 2002 2:46 pm Operator: Sample : re-ext. Inst : 1netrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 20 1,3,5-Triazine, 2,4,6-trime... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.90 0.46 ug/L 264605 Perylene-dl2 34.65

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 1,3,5-Tkiazine, 2,4,6-trimethyl- 123 C6H9N3 000823-94-9 9 2 Heptanoic acid, 3-hexenyl ester,... 212 C13H24O2 061444-39-1 9 3 Pentanoic acid, 5-hexen-l-yl ester 184 C11H20O2 1000159-23-9 9 4 7-Hexadecyn-1-ol 238 C16H30O 000822-21-9 9 Abundance Scan 5415 (34.896 min): 12763.D (-5414) (-) m/z 260.05 100.00% 67 82 116 2(0

208 5000 44 i . ( । । । ’TT 1 1 > | r-r-r l । . . 130 281 34.60 34.80 35.00 35.20 OPPITT ' ‘ I ' ’1 * I 1 97 T11 TT 1' i ■ ■'' i' ■ ■11 ■ ■' ■ i ' ■ ■ i ■ ■ ■ • i ■ ■ I ■ ■ i ■ ■ m/z 67.10 85.90% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32314:1,3,5-Triazine, 2,4,6-trimethyl- 42 82 123 f

5000 34.60 34.80 35.00 35.20 m/z 116.00 84.14% 15 67 ___ 0- I . ■ ■ i'" . .1 .1 i ’ ■1 • i ■ ■1 ■ i ■ ■ ■ ■ । •1 ■ ■ i i ■ ■ ■ 11 ■ ■ ‘ ■ i ‘1 ■ 11 •1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32451: Heptanoic acid, 3-hexenyl ester, (Z)- 43 67 82 34.60 34.80 35.00 35.20 5000 m/ Z 82.10 83.70% 29 113

131 0- ■ ■ ।,T ri’ — M | m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #21544: Pentanoic acid, 5-hexen-1-yl ester i ■ rt"i j ■ • i ' ' । 67 85 34.60 34.80 35.00 35.20 54 m/z 85.10 81.06% 41 ...... 5000

27 103

n/z-> 0 20 MV ++ i""I , | " 1 rt ' 1" 1 127 143 60 80 100 120 140 160 180 200 220 240 260 280 40 1 f"'1 i ■ ■ ' ■ i ■ i ■ ■ ■' । ■ ■ ■ ■ । ■ 71 " I ■ ' • 34.60 34.80 35.00 35.20 114 1 '

12763.D 060302.M Tue Jun 11 15:54:25 2002 Page 23

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