GCMS analysis report, sample AE12763, June 2002

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Data File C:\MSDCHEM\1\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 15 Borane, trifluoro- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 4.97 0.50 ug/L 429258 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW Mol Form CAS# Qua

1 Borane, trifluoro- 68 BF3 007637-07-2 A 2 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 2 3 Ethyl Chloride 64 C2H5C1 000075-00-3 2 4 2-Chloroethanol 80 C2H5C10 000107-97-3 2 Abundance Scan 321 (4.965 min): 12763.D (-318) (-) m/z 49.10 7100.00% 49

5000 84 41 4.60 4.80 5.66 5.20 ' 5.40 m/z-> 0- 0 phila —50m***2PPP ■ i ■ ■ ■ ■ i ■ 10 20 30 40 60 35 70 80 H I 90 100 110 120 130 m/ Z 51.00 67.48% Abundance #12321: Borane, trifluoro- 49

5000 4 60 4.80 5.00 5.20 5.40 m/z 84.00 41.53% 0- 1,1 19 ' I1' ■' ■'!' 30 38 TIT i11 ■ ■ i ■ 68............................ miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1099: Boron trifluoride etherate 31 59 4 60 4.80 5.00 5.20 5.40 5000 45 m/z 48.05 26.38% 74 "...

0- *11 1 454254 1 +3944— Hritt 66 r 81 93 127 niz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #107943: Ethyl Chloride 23 4 60 4.80 5.00 5.20 5.40 m/z 41.10 . 22.35%

Muirsa 64 5000

49 15 35 0- 1 1 1 1 I Mll, 1 । 1 1 t' 1+ isan, ■' ' ml -rYT-r-rrTT-r-r-r-p-r-r-r-p-r-r-r-p-r-r-ry-^^ /z-> o 10 20 30 40 50 60 70 80 90 100 110 120 130 4.60 4.80 5.00 5.20 5.40

12763.D 060302 .M Mon Jun 10 10:29:09 2002 Page 18

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