GCMS analysis report, sample AE12763, June 2002

NYC 9/11 Public Portal Document LLDLCLY DedrcI compound Keporc

Data File C:\MSDCHEM\1\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 Borane, trifluoro­ Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.25 4.10 ug/L 3499920 1,4-dichlorob'enzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Borane, trifluoro- 68 BF3 007637-07-2 / 2 Ethanol, 2,2,2-trifluoro- 100 C2H3F30 000075-89-8/1 3 Ethanol, 2,2,2-trifluoro- 100 C2H3F30 000075-89-8 1 4 2-Chloroethanol 80 C2H5C1O 000107-0773 1 Abundance Scan 199 (4.248 min): 12763.D (-196) (-) m/z 49.10 100.00% 49

5000 44 73 36 85 4.00 4.20 4.40 4.60

niz-> 0- 0 10 / 20 ........ 30 I|li 40 50 ■ i ‘ ■ i ■ * • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ' ■ ■ i ■ ■ 60 70 80 90 100 m/z 47.00 50.08%

Abundance #12321: Borane, trifluoro- 49

5000 4.00 4.20 4.40 4.60 m/z 73.10 26.70% 11 19 30 38 68 0- **1***IIa*’1IIIII i ■ ■ ■ ■ i ■ ■ ■ I I ■ ■ ■ ■ i ' ■ 1 > i ■ ■ ■ ■ i ■ ■

m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #108313: Ethanol, 2,2,2-trifluoro- 31 4.00 4.20 4.40 4.60 5000' m/z 44.00 26.06% 61 51

miz-> 0- 0 13 19 26 —4— 1’11/4/4/1/14/4 ' -T'1. ■ 10 20 30 40___ 50 60 69 | TI——————mTTT 70 80 90 pi 81 100 100

Abundance #1043: Ethanol, 2,2,2-trifluoro- 31 4.00 4.20 4.40 4.60 m/z 36.10 19.97% 5000

61 51 0- — ———14 19 26 ————H IITi' 441 ■ ‘..I 69 81 100 'I1' i ■ ■ I1'1' ' 1 T ' 1 1 Ul’tml 1111 miz-> 0 10 20 30 40 50 60 70 80 90 100 4.00 4.20 4.40 4.60

12763.D 060302.M Mon Jun 10 10:29:07 2002 Page 15

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