GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document LIDLCL DtdLCil toupOu KCDOLU

Data File C:\MSDCHEM\1\DATA\060702\12742.D Vial: 16 Acq On 7 Jun 2002 8:47 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Borane, trifluoro- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.88 1.50 ug/L 984628 1,4-dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Borane, trifluoro- 68 BF3 007637-07-2 2 1-Propanol, 3-chloro- 94 C3H7C1O 000627-30-5 3 2-Chloroethanol 80 C2H5C1O 000107-07-/ 2 4 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-3 9 2 Abundance Scan 137 (3.884 min): 12742.D (-135) (-) m/ z 49.10 0.00% 49

5000 35 84 42 3.60 3.80 4.00 4.20 Of 10’0’1211101311111111112—1211777 T 1"" m/z 84.00 25.32% mfz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #12321: Borane, trifluoro- 49

5000 ‘ ‘i • ‘ * i * * ' 1 i r‘ ' * i 1 4 3.60 3.80 4.00 4.20 m/z 35.10 23.58%

n/z—> Abundance 0- ———————— 11 1? 30 38 i"" i" "i 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 68 ■i" ''I" "i"111" "i

#108340:1-Propanol, 3-chloro- ■ i" " i" " i" " 1

W "W Mu 3h

58 3.60 3.80 4.00 4.20 5000

0b ^“‘*1’’’’I — 26 41 +.3f,1 111118.117 ,11"63111168 76 93 "11" “ 1111' I"111111'i1r" 111" i11111 m/z

Vw/ PyAamua, 48.10 20.81%

" miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #108293:2-Chloroethanol 31 3.60 3.80 4.00 4.20 m/z 50.00 16.69% 5000

36 43 49 61 80 M„/Aula Of■ ■1 ■ i ■1 • ■ i ■ ■' ■ i'1 ■' i' ■ ■' i ■ TT———Tp m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 3.60 3.80 4.00 4.20

12742.D 060302.M Mon Jun 10 11:26:28 2002 Page 8

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