GCMS quantitation report, sample AE11933, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report • Data File : C:\MSDCHEM\l\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L

Peak Number 8 l-Buten-3-yne Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.95 0.42 ug/L 345661 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual l l-Buten-3-yne 52 C4H4 000689-97-4 5 2 l-Buten-3-yne 52 C4H4 000689-97-4 5 3 l-Buten-3-yne 52 C4H4 000689-97-45 4 Ethyl Chloride 64 C2H5C1 000075-00-3 4 Abundance Scan 148 (3.949 min): 11933.D (-146) (-) m/z 87.95 100.00% 49 83 — 43

5000 83

3640 57 3.60 3.80 4.00 4.20 mmmmHHHH 01 ‘1’1 -TTTTTTT — ■I'‘‘'i'' m/z 49.10 •88.45% miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111078:1-Buten-3-yne 52

5000 ■ ■ i - ' ■ ■ i 1 ■ ■ ■ i ■ ■ ' ■ i ■ ' ■ ■ i ' 3.60 3.80 4.00 4.20 m/z 43.10 71.50% 2 12 1 37 48 *mmmWPLWmWPL?PWTPTRTTTTT 0- * * • >।>।" i>•*>i ■ > k i >■" i ■■>>|lt । • j1 11> 111 nl>।■i* ■11 niz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111077:1-Buten-3-yne 52 T IT 3.60 3.80 4.00 4.20 5000 m/z 51.90 50.12%

37 48 2629 n/z-> 0- 2 mH 12 "" i ““i “ ■ ■ i' ‘“i" hmmmpmmmmppt 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12456:1-Buten-3-yne fit $ 3.60 3.80 4.00 4.20 m/z 82.90 44.23%

5000

26 „ WMWH4k 0 ,1, TTTITTTI)mmmTLTTTT 37 48 —pr iz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

11933.D 060302.M Tue Jun 11 08:23:11 2002 Page 11

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