Report documenting the recovery percentage of the 2,4-DDD surrogate standard used to validate gas chromatography-mass spectrometry analysis.
NYC-WTC_000015696–000015724Folder label: “GCMS X 6/7/02 A 6/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\0610022\12283.D Vial: 11 Acq On : 10 Jun 2002 7:10 pm Operator: Sample : gc/ms scan 6/7 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Thiophene, 2-[2-(3-thienyl)... Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.27 ug/L 325946 Phenanthranene-dl0 22.91
Hit# of 5 Tentative ID MW ■ MolForm CAS# Qual
1 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 50 2 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H12O3 1000132-15-8 50 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5/45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 Abundance Scan 3311 (22.533 min): 12283.D (-3291) (-) m/z 192.00 100.00% 19/2
5000
96 146 160 ..... a.... Ai 22.20 22.40 22.60 22.80 ' ~' mfc-> 42 51 66 82 I | | l 0 ' l ' • " I " 1' I 11 ' 1 1'" “ m I I | I I ■ I | I I I I 11 I I I | , I , I rrri i 11 i > i । i ■ n-j-rr+rj > i i ifrrr. । i i , i । , i i i j1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.00 21.62% Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 192
147 5000 22.20 22.40 22.60 22.80 45 m/Z 193.10 14.68%| 1 58 69 ro 96 115 iz-> 27 0: TITTTTT -----+99-+ H ■ i ■ 177 i ■ ■ “ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 134 , 158 . I Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid A 192 ....................................... "T 22.20 22.40 22.60 22.80 5000 m/z 96.10 14.31% 175 63 89 45 1 77 117 145 105 1 7 135 I 0 -----4+4,++4,Tptmtnmpmm 163 I miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-DihydrophosphoIe, 3-methyl-1-oxo-1 -phenyl- 19 2 22.20 22.40 22.60 22.80 164 m/z 146.10 13.45%| 5000 99 115 47 77 177 67 125 146 0 .44 li57 ,II, , 87,41444p4.34 4155, TTTdm hajondpanna] -r-p-r . ...... A n/z—> 20 30 40 50 60 70 - 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80
12283.D 060302.M Tue Jun 11 08:24:53 2002 Page 22
NYC-WTC_000015722
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NYC-WTC_000015651
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 11, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015741
Quantitative analysis report for polycyclic aromatic hydrocarbons using gas chromatography-mass spectrometry from June 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014433
Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015725
Quantitative analysis report for polycyclic aromatic hydrocarbons using gas chromatography-mass spectrometry from June 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014406
Laboratory report showing GCMS analysis results for sample AE12476 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015224
Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014552
Laboratory report showing GCMS analysis results for sample AE12533 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015282
Laboratory report documenting GCMS analysis of sample AE12738 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015171
Laboratory report listing reference values for volatile organic compounds in sample AE12735 with associated numerical data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014384
Laboratory report showing GCMS analysis results for sample AE12326 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014460
Laboratory report showing GCMS analysis results for sample AE12478 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014509
Laboratory report showing GCMS analysis results for sample AE12531 including surrogate recovery data on June 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
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NYC-WTC_000015648
Gas chromatography-mass spectrometry analysis report for sample AE12676 detecting unknown compounds and surrogates on June 6, 2002.
Filed in the same folder
NYC-WTC_000015649
Record of liquid extractor drip rates and pH values for sample processing at the Department of Environmental Protection laboratory.
Filed in the same folder
NYC-WTC_000015651
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 11, 2002.
Filed in the same folder
NYC-WTC_000015679
Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 11, 2002.
Filed in the same folder
NYC-WTC_000015683
Reference standard analysis report for volatile organic compounds using gas chromatography-mass spectrometry on June 11, 2002.
Filed in the same folder