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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12737 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015253–000015281

Folder label: “GCMS X 6/3/02 A 6/7/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary

• Operator ID: Date Acquired: 7 Jun 2002 7:10 pm Data File: C:\MSDCHEM\l\DATA\060702\12738.D Name: Mise: Method: C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Butanoic acid, me... 3.47 0.3 ug/L 150881 1 9.89 23236100 40.0 Methylene Chloride 3.73 12.2 ug/L 7089290 1 9.89 23236100 40.0 Ethane, 1-chloro-... 3.79 2.4 ug/L 1413400 1 9.89 23236100 40.0 2-Amino-oxazole 3.81 6.3 ug/L 3638540 1 9.89 23236100 40.0 Aspartic acid 3.87 19.1 ug/L 11122100 1 9.89 23236100 40.0 Methylene Chloride 4.11 13.3 ug/L 7726410 1 9.89 23236100 40.0 l-Buten-3-yne, 2-... 4.30 2.7 ug/L 1563160 1 9.89 23236100 40.0 Piperidine, 2-pro... 4.36 1.3 ug/L 727930 1 9.89 23236100 40.0 1-Propene, 2-meth... 4.40 6.3 ug/L 3631970 1 9.89 23236100 40.0 l-Penten-3-one 4.67 1.7 ug/L 1008020 1 9.89 23236100 40.0 2-Butyne-1,4-diol... 4.72 1.0 ug/L 592501 1 9.89 23236100 40.0 2-Butenal, 3-methyl- 4.80 2.1 ug/L 1199930 1 9.89 23236100 40.0 Acetaldehyde, dim... 4.87 1.4 ug/L 805799 1 9.89 23236100 40.0 2-Fluoroimidazole 5.40 0.4 ug/L 206456 1 9.89 23236100 40.0 Ethanol, 2,2-dich... 5.82 0.3 ug/L 164215 1 9.89 23236100 40.0 2-Pentanone, 4-hy... 5.95 0.6 ug/L 362709 1 9.89 23236100 40.0 Butane, 2,2,3,3-t... 8.70 0.3 ug/L 191615 1 9.89 23236100 40.0 Cyclopentasiloxan... 12.37 0.3 ug/L 210819 2 13.39 31431700 40.0 Anthracene-dlO- 23.06 0.3 ug/L 300569 4 22.90 35885700 40.0 Dibutyl phthalate 25.05 0.9 ug/L 771231 4 22.90 35885700 40.0

12738.D 060302.M Mon Jun 10 11:45:49 2002 Page 24

NYC-WTC_000015281

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NYC-WTC_000015281Source: NYC Law Department, mirrored locally

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