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GCMS blank analysis results, May 22, 2002

Machine-extracted title · confidence 95%

Laboratory report showing blank sample analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.

NYC-WTC_000013049–000013076

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary .’operator ID: Mclean Date Acquired: 21 May 2002 8:40 pm Data File: C:\MSDCHEM\1\DATA\052102\LB.D Name: Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Methylene Chloride 3.69 0.7 ug/L 548700 1. 9.90 31366100 40.0 Crotonic acid 3.71 1.1 ug/L 859037 1 9.90 31366100 40.0 2-Butenal, 2-methyl- 3.76 0.8 ug/L 622002 1 9.90 31366100 40.0 Borane, trifluoro- 3.82 0.9 ug/L 693652 1 9.90 31366100 40.0 2-Butenal, 3-methyl- 3.85 0.4 ug/L 343132 1 9.90 31366100 40.0 Thiophene 3.87 0.6 ug/L 468404 1 9.90 31366100 40.0 Krypton 3.91 0.3 ug/L 259274 1 9.90 31366100 40.0 Methylene Chloride 4.20 0.6 ug/L 435891 1 9.90 31366100 40.0 Toluene 4.28 0.8 ug/L 648880 1 9.90 31366100 40.0 N-(2-Acetylcyclop... 5.38 0.2 ug/L 158563 1 9.90 31366100 40.0 2-Pentanone, 4-hy... 5.94 10.1 ug/L 7956390 1 9.90 31366100 40.0 Phenanthrene, 9-m... 22.54 0.3 ug/L 333446 4 22.91 46998900 40.0 Anthracene-dl0- 23.07 0.3 ug/L 324966 4 22.91 46998900 40.0 Trisiloxane, 1,1,... 32.00 0.2 ug/L 222991 5 30.77 42331600 40.0 Cyclononasiloxane. .. 33.20 0.8 ug/L 596078 6 34.67 31127900 40.0 Cyclononasiloxane. .. 34.33 1.2 ug/L 947900 6 34.67 31127900 40.0 Cyclononasiloxane. .. 35.38 1.5 ug/L 1136330 6 34.67 31127900 40.0 Cyclononasiloxane. ... 36.45 1.6 ug/L 1211920 6 34.67 31127900 40.0 Cyclononasiloxane. .. 37.72 1.2 ug/L 932703 6 34.67 31127900 40.0 Cyclononasiloxane. .. 39.27 0.9 ug/L 687347 6 34.67 31127900 40.0

LB.D 052202.M Wed May 22 12:03:25 2002 Page 24

NYC-WTC_000013076

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NYC-WTC_000013076Source: NYC Law Department, mirrored locally

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