GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document ulprary earcn compound Keporc

Data File C:\MSDCHEM\1\DATA\060702\12738.D Vial: 14 Acq On 7 Jun 2002 7:10 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 2-Fluoroimidazole Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 5.40 0.36 ug/L 206456 1,4-dichlorobenzene-d4 9.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Fluoroimidazole 86 C3H3FN2 1000129-59-1/4 2 2-Butenoic acid, (E) - 86 C4H602 000107-93-7/4 3 5-Fluoroimidazole 86 C3H3FN2 1000128-06-0 4 4 1,2-Ethanediamine, N,N,N‘-triethyl- 144 C8H20N2 000105-04-4 4 Abundance Scan 395 (5.400 min): 12738.D (-393) (-) 86.00 100.00% 85 35

47 51 41 5000

44 5.00 5.20 5.40 5.60 5.80 -H 0 i ■ ■ ■ ' 111 1- m/z 35.10 82.46% niz-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34865:2-Fluoroimidazole 85

5000- 5.00 5.20 5.40 5.60 5.80 59 m/z 47.00 59.65% 41 44 51 55 64 67 71 01 I 1 1 ‘ 1 1 1 1 " I " " I 1 1 "I Mnpi.ll.il i • > * > I ■ ।• I > > ■ > l >1 ■ * 1111 ■ l --- n/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116768:2-Butenoic acid, (E)- 85 ■ i ■ 1 1 ■ i 1 ■ 41 5.00 5.20 5.40 5.60 5.80 5000 m/z 51.10 59.65% 69 45 38 0 -34 1,. 50 53 57 60 63 66 72 75 11111■!■ ■ ।■ i.11■ i~...।!11r...।. TPTH 1111" 1111' n/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34861:5-Fluoroimidazole ■ i • ‘ ■ i ■ ■ ■ ■ i ■ • • • i ■ 1 ■ ■ i ■ 1 85 5.00 5.20 5.40 5.60 5.80 m/z 41.00 51.75% 5000 59

,41 44 51 55 66 69 83 0 1 I ' ' ' 1 I 1 ' 1 1 | . . . . । . > . if . r . . | I iz-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60 5.80

12738.D 060302.M Mon Jun 10 11:45:45 2002 Page 17

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