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Document / 8 pages

GCMS reference analysis results for volatile organics, June 2002

Machine-extracted title · confidence 90%

Laboratory report displaying calibration percentages for various volatile organic compounds including nitrosamines and chlorobenzenes.

NYC-WTC_000015163–000015170

Folder label: “GCMS X 6/3/02 A 6/7/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\060 7 02\REF1.D Vial: 9 Acq On 7 Jun 2002 3:06 pm Operator: Sample gc/ms scan 6/3 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 10 11:12:27 2002 Quant Results File: 060302.RES Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu Jun 06 15:03:45 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.49 202 7882379 16.63 ug/L 99 3 8) Pyrene 27.12 202 8121435 16.61 ug/L 98 39) Butylbenzylphthalate 29.47 149 1939816 16.45 ug/L 96 40) Benzo(a)anthracene 30.73 228 4892951 14.20 ug/L 100 41) Bis(2-ethylhexyl)phthalate 31.34 149 1834524 15.88 ug/L 97 42) Chrysene 30.82 228 6052569m 16.53 ug/L 44) Di-n-octylphthalate 33.17 149 1341177m 16.92 ug/L 45) Benzo(b)fluoranthene 33.70 252 2990428 12.56 ug/L 98 4 6) Benzo(k)fluoranthene 33.77 252 4906994 17.16 ug/L 99 47) Benzo(a)pyrene 34.50 252 2588640m 11.39 ug/L 48) Indeno(1,2,3-cd)pyrene 37.32 276 883937 5.76 ug/L 97 49) Dibenz(a,h)anthracene 37.43 278 1505667 8.93 ug/L 100 50) Benzo(g,h,i)perylene 38.05 276 2061743 11.45 ug/L 93

(#) = qualifier out of range (m) = manual integration (+) = signals summed REFl.D 060302.M Mon Jun 10 11:14:16 2002 Page 2

NYC-WTC_000015169

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NYC-WTC_000015169Source: NYC Law Department, mirrored locally

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